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2.
Saier Liu Guangxiao Li Minjing Shang Zheng-Hong Luo Yuanhai Su 《American Institute of Chemical Engineers》2021,67(11):e17362
Hydrodynamics characteristics of a fast and highly exothermic liquid–liquid oxidation process with in situ gas production in microreactors were studied using a newly developed experimental method. In the adipic acid synthesis through the K/A oil (the mixture of cyclohexanol and cyclohexanone) oxidation with nitric acid, bubble generation modes were divided into four categories. The gas production became more intensive, unstable, even explosive with increasing the oil phase feed rate and the temperature. A novel automatic image processing method was developed to monitor the instantaneous velocity online by tracking the gas–liquid interface. The axial velocity at the same location was unstable due to the changing gas production rate. Furthermore, the actual residence time was obtained easily with being only 36% of the space–time minimally, beneficial for establishing accurate kinetics and mass transfer models with time participation. Finally, an empirical correlation was developed to predict the actual residence time under different conditions. 相似文献
3.
Xufen Xie Yingying Shang Jieyu Zhu Ningfang Liao Wenmin Wu Jing Liang Chaoqun Fu 《Color research and application》2021,46(1):65-74
Reconstruction of spectral information based on multi‐channel image system is a significant problem in color reproduction, detection, and recognition. A spectral radiance reconstruction from trichromatic digital camera responses is researched in this article. The mapping relationship between the trichromatic imaging system response and the incident spectral radiance is analyzed. Then, in order to remove the ill‐posedness of the problem, a regularized constraint solution model of spectral radiance reconstruction matrix is established. And the spectral radiance can be reconstructed by spectral radiance reconstruction matrices and trichromatic imaging system response. Finally, the spectral radiance reconstruction matrix is estimated by the system radiometric calibration experiment. The input radiance is offered by a LCD display. A 3‐factor and 9‐level orthogonal test is designed for the calibration experiment, and a test set of 24 colors is used for precision analysis. The results show that the average relative mean error of our method is 8.69%, it is lower than that of Wiener filtering method by 2.84%. The method can reconstruct spectral radiance information effectively. 相似文献
4.
采用高温固相法制备了CaY2-xLuxAl4SiO12:0.006Mn4+ (x=0,0.6,1,1.4,2)荧光粉.研究了Y/Lu组份的变化对荧光粉的晶体结构和发光性能的影响.研究发现,随着Lu组份的增多,荧光粉的吸收峰和发射峰位置都出现蓝移.研究了Mn4+掺杂浓度对CaLu2Al4SiO12∶yMn4+发光性能的影响,发现在掺杂浓度为y=0.004时出现了浓度猝灭现象,浓度猝灭是由Mn4+之间的电偶极电偶极相互作用引起的.研究了不同Mn4+掺杂浓度的CaLu2Al4SiO12∶Mn4+荧光粉的荧光寿命,荧光寿命随着Mn4+掺杂浓度的增大而逐渐降低. 相似文献
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目的 在视觉引导的工业机器人自动拾取研究中,关键技术难点之一是机器人抓取目标区域的识别问题。特别是金属零件,其表面的反光、随意摆放时相互遮挡等非结构化因素都给抓取区域的识别带来巨大的挑战。因此,本文提出一种结合深度学习和支持向量机的抓取区域识别方法。方法 分别提取抓取区域的方向梯度直方图(HOG)和局部二进制模式(LBP)特征,利用主成分分析法(PCA)对融合后的特征进行降维,以此来训练支持向量机(SVM)分类器。通过训练Mask R-CNN(regions with convolutional neural network)神经网络完成抓取区域的初步分割。然后利用SVM对Mask R-CNN识别的抓取区域进行二次分类,完成对干扰区域的剔除。最后计算掩码完成实例分割,以此达到对抓取区域的精确识别。结果 对于随机摆放的铜质金属零件,本文算法与单一的Mask R-CNN及多特征融合的SVM算法就识别准确率、错检率、漏检率3个指标进行了比较,结果表明本文算法在识别准确率上较Mask R-CNN和SVM算法分别提高了7%和25%,同时有效降低了错检率与漏检率。结论 本文算法结合了Mask R-CNN与SVM两种方法,对于反光和遮挡情况具有一定的鲁棒性,同时有效地提升了目标识别的准确率。 相似文献
8.
Xianwei Su Xiaojia Shang Yusi Che Shaolong Li Jianxun Song Jilin He 《Ceramics International》2021,47(15):21459-21465
Homogenous ZrCxOy powders have been successfully synthesized by in-situ electro-reduction of solid ZrO2–C composite precursors in molten CaCl2. The effect of applied cell voltage and molar ratio of ZrO2 to C on preparation of ZrCxOy were investigated. The reduction pathway of the composite electrode was studied based on the analysis of intermediate products using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The results show that ZrO2 is firstly converted to CaZrO3. The resulting CaZrO3 is then reduced to ZrCxOy. The ZrCxOy formation is dramatically influenced by electrolysis voltage and molar ratio of ZrO2 to C: a higher cell voltage and lower molar ratio of the ZrO2 to C are more preferable for the formation of ZrCxOy powder. Homogenous ZrCxOy powders with particle size of ~100 nm are synthesized by ZrO2/C starting elemental powders in CaCl2 molten salt at 1123 K for more than 3 h, when the cell voltage is 3.0 V and the molar ratio of the ZrO2 to carbon starting materials is 1:1.0. 相似文献
9.
为确定半干旱地区膜下滴灌条件下玉米生长与土壤含水量间的关系,利用通榆灌溉试验站2018年度玉米膜下滴灌灌溉制度试验数据,分析不同灌溉制度下的玉米产量,并对不同灌溉制度下的玉米株高、茎粗、叶面积等指标进行回归求解,得到了玉米各生育阶段的适宜土壤含水量及其阈值.玉米膜下滴灌各生育阶段的适宜土壤含水量区间:苗期65%—75%、拔节期70%—80%、抽雄吐丝期75%—85%、灌浆期75%—85%、乳熟期70%—80%;水分胁迫阈值:苗期50%、拔节期57%、抽雄吐丝期66%、灌浆期60%、乳熟期58%. 相似文献
10.
Long Zhao Xu Xu Jing-Bin Lu Ya-Lin Gong Xiang-Lin Li Wei Zhang Qing-Min Shang Qing-Feng Song Yan-Feng Li 《核技术(英文版)》2019,30(4)
A prompt gamma-neutron activation analysis(PGNAA) system was developed to detect the iron content of iron ore concentrate. Because of the self-absorption effect of gamma-rays and neutrons, and the interference of chlorine in the neutron field, the linear relationship between the iron analytical coefficient and total iron content was poor, increasing the error in the quantitative analysis. To solve this problem, gamma-ray self-absorption compensation and a neutron field correction algorithm were proposed, and the experimental results have been corrected using this algorithm. The results show that the linear relationship between the iron analytical coefficient and total iron content was considerably improved after the correction. The linear correlation coefficients reached 0.99 or more. 相似文献